Tips and hints are provided for specific applications, and the measurement fundamentals are backed up in a theoretical part. Checking membrane a sqall hole of any size on the membrane or breakage of the membrane causes failure of the electrode. These are general instructions which can be used with most meters to check the. Design of ion selective electrodes solid state electrodes. Prepare the meter according to the meter user guide. High performance ammonia electrode user guide 1 general information introduction the. Chloride ion selective electrode theory, practice and. The following is a description of these techniques. The accumet line includes benchtop and portable meters as well as a complete offering of electrodes to meet a wide range of laboratory needs. Flexible groundjoint diaphragm for measurementtitration with ion selective electrodes routine measurement of samples of identical composition, ph 1 11 ceramic pin diaphragm skin surface measurement. Chloride electrode, chloride ise, chloride ion selective. The chloride sensors electrode uses a permafil nonrefillable, ion selective electrode. The chloride ion selective electrode is intended for measuring chloride ion concentrations and activities in aqueous. We offer a comprehensive portfolio of ion selective electrode calibration standards, ionic strength adjusters, reagents, and fill solutions for your ise measurement needs.
Required equipment checking electrode operation slope. This user guide contains information on the preparation, operation and maintenance for the fluoride ion selective electrode ise. The analyzer provides automatic, online monitoring based on ion selective technology analysis. Cupric ion selective electrode thermo fisher scientific. When the reading is stable, set the meter to the ph value of the buffer at the measured temperature. Chloride ionselective electrode user manual vernier. Make sure that both orings are in place on the module. The stock solutions described in this section may be created as described or ordered directly from pasco. A phmv meter or an ion meter, either line operated or portable. Thermo scientific ise user manual pdf download manualslib. User manual for the auto analyser can be downloaded from here. Fill the 900200 double junction reference electrode according to instructions in the reference electrode user guide. They also are suitable for use with any other ion meter, or with any meter with 0.
It is recommended to check the membrane on every newly assembled electrode. The vernier chloride ion selective electrode is used to measure the concentration of. Lead ion selective electrode user guide 5 electrode setup electrode preparation 9482bn and 9482sc lead halfcell electrode remove the protective shipping cap from the sensing element and save the cap for storage. The membrane must be insoluble in the analyte solution and contain the analyte ion of interest. Screw the sensing module into the 93 series electrode. The electrode is shipped without filling solution in. The chloride ise has a combinationstyle, nonrefillable, gelfilled electrode.
All refillable agagcl ph electrodes have a ph range of 0 to 14 and silversilver chloride reference system. Remove the sensing module from the vial and save the vial for storage. General analytical procedures, electrode characteristics and electrode theory are also included in this user guide. Fisher scientific accumet meters have been leading the way in electrochemistry design and functionality since 1965. Refillable agagcl ph electrode user guide introduction this user guide contains information on the preparation, operation and maintenance of the thermo scientific orion refillable agagcl silversilver chloride ph electrodes. The vernier chloride ionselective electrode ise is a membranebased electrode that measures a specific ion cl in an aqueous solution. Thermo scientific orion ion selective electrode selection. Fluoride ion selective electrode user guide 5 electrode setup electrode preparation 9409bn and 9409sc fluoride halfcell electrode remove the protective shipping cap from the sensing element and save the cap for storage. Sodium electrodes can be used on any ise meter with a bnc connection. Thermo scientific 9417bn chloride electrodes tequipment. The electrodes can also be used on meters with a variety of inputs when an adapter cable. Slope is defined as the change in millivolts observed with every tenfold change in concentration.
Ion selective electrodes guide theory, practice and. Thermo scientific orion fluoride ion selective electrode. This ise has to be used in combination with a reference electrode and is suitable for. An ion selective membrane prevents the reaction of sodium hydroxide and hydrogen with chlorine.
Our products are not designed nor are they recommended for any industrial, medical, or commercial process such as life support, patient diagnosis, control of a manufacturing process, or industrial testing of. Direct calibration is a simple procedure for measuring a large number of samples. Standard ammonia ion selective electrode user guide introduction this user guide contains information on the preparation, operation and maintenance for the ammonia ion selective electrode ise. Chloride ionselective electrode instruments direct. The 900100 reference electrode is a sleevetype refillable agagcl silversilver chloride reference electrode designed for precision measurements with ion selective halfcell. Ion selective electrode startup and calibration guide. When the membrane of the electrode is in contact with a solution containing the specific ion, a voltage, dependent on the level of that ion in solution, develops at the membrane. Before analysis units of measurement sodium can be measured in units of moles per liter, parts per million, % salt, mgserving, or any other convenient unit depending. Make sure that the rubber electrode washer on the sensing module is in place. Its preferred applications are to be found in the field of water, sauces, health drinks, soil, salad dressings, mayonnaise analysis etc.
Do not to touch the sensing membrane or reference pellet during the electrode assembly. If the electrode has been stored dry, prepare the electrode as. Thermo scientific orion ion selective electrodes thermo. Unlike other ises available from vernier, the chloride ise has a solidstate membrane that does not need to be replaced. Oct 14, 2017 b differences between ph and other ion selective electrodes. Ionselective electrode monitor model 8232 ammonia monitor special range 0. Salt analysis, manual titration, canned vegetables, food analysis, titration of chloride. Chloride selective electrode with crystal membrane. This user guide contains information on the preparation, operation and maintenance for the chloride ion selective electrode ise. The chloride ion selective electrode is intended for measuring chloride ion concentrations and activities in aqueous solutions. Measuring salt content in canned vegetables using manual. Use the chloride ise to measure chloride levels in ocean saltwater or salt in food samples. Obtaining the slope value provides the best means for checking electrode operation.
Page 16 fluoride ion selective electrode user guide. This ion selective electrode guide focuses on giving practical description of how to measure ions selectively in the laboratory. Ion selective electrodes thermo scientific orion ion selective electrode selection guide species cat. Chloride electrodes measure free chloride ions in aqueous solutions. Rinse the electrode first with distilled water and then with the buffer being used for calibration. The membrane consists of a solid salt of silver sulfide silver chloride ag 2 s agcl. Double junction makes these electrodes ideal even for rugged applications. Aug 14, 2015 the chloride ionselective electrode has a solidstate polycrystalline membrane. For use with equipment chloride electrodes can be used on any ise meter with a bnc connection the electrodes can also be used on meters with a variety of inputs when an adapter cable is used. Iodide ion selective electrode user guide 5 checking electrode operation slope these are general instructions that can be used with most meters to check the electrode operation.
Chlorine is also produced in a number of other ways, for example, by electrolysis of potassium chloride brine in membrane and mercury cells with coproduction of potassium hydroxide. This solution also contains the same ions as that to be measured. Within this ion selective electrode, there is an internal reference electrode, which is made of silver wire coated with solid silver chloride, embedded in concentrated potassium chloride solution filling solution saturated with silver chloride. Construction measurement range optimum temperature range required reference electrode reference filling solution calibration standards required isa ammonia standard nh 3 9512bnwp 1 gas sensing combination 5 x 107 to 1. Download manual pdf go direct chloride ionselective electro deise is used to measure the concentration of chloride cl. Go direct chloride ionselective electrode user manual vernier.
Chloride ion selective electrode user guide general information introduction this user guide contains information on the preparation, operation and maintenance for the chloride ion selective electrode ise. Fluoride electrodes measure free fluoride ions in aqueous. Guidebooks for instructions on transferring datamate to the calculator. Metal electrodes digital general chloride, table salt content in foods determination of hydrogen sulfide, mercaptans, carbon sulfides. Fluoride ion selective electrode user guide 1 introduction this user guide contains information on the preparation, operation and maintenance for the fluoride ion selective electrode ise. Use these economical ion selective electrodes ises with the ion 510 meter, ph 2500 ion benchtop meter, or the ion acorn meters. Thermo scientific orion ion selective electrodes thermo scie. Chloride ions are found in freshwater samples as a result of water flowing over saltcontaining minerals. The electrode is designed for the detection and analysis of chloride ions in aqueous. Chloride ion electrodes instruction manual general instructions introduction the coleparmer chloride ion electrodes are used to quickly, simply, accurately, and economically measure chloride ions in aqueous solutions.
It is designed to be used with the vernier go direct ise amplifier order code gdxisea. Chloride combination ion selective electrode hi4107. Ion selective electrode analysis chemistry libretexts. Download manual pdf go direct chloride ionselective electrode ise is used to measure the concentration of chloride cl. Fluoride ion selective electrode user guide checking electrode operation slope these are general instructions that can be used with most meters to check the electrode operation. This user guide contains information on the preparation, operation and maintenance for the residual chlorine ion selective electrode ise. The concentration of the chloride ion gives a quick measurement of salinity of water samples.
The chloride ise should not be used in solutions containing high concentrations of bromide or. Analytical techniques analytical techniques a variety of analytical techniques are available to the analyst. This model includes a reference electrode and an ion selective electrode selective for monovalent fluoride ions. Thermo fisher scientific user guide indomultimeter. Goal the following application note describes how to reliably measure the salt content in canned vegetables by manual titration to mv endpoint using a thermo scientific orion chloride ion selective electrode ise or a. The ion selective electrodes are part of a group of relatively simple and inexpensive analytical tools which are commonly referred to as sensors. Connect the ise to a meter that can directly display ion concentration e. The main characteristic of a solid state electrode is that the sensing material is almost insoluble in water, meaning a very small solubility product. Determination of chloride using potentiometry chemistry. Chloride ion selective electrode user guide fisher scientific. Chloride ion selective electrodes omega engineering. Results provide the information needed to operate your power plant with a high level of reliability and efficiency. The ph electrode is the most wellknown and simplest member of this group and can be used to illustrate the basic principles of ises. Fixed position, glass sensor bulb if the electrode slope is not within the normal range, the size and material.
These are general instructions that can be used with most. Chloride ion selective electrode user guide using the electrode electrode preparation 94 7bn and 94 7sc chloride halfcell electrodes 1. The vernier chloride ionselective electrode is used to measure the concentration of chloride cl. Standard ammonia ion selective electrode user guide. Ion selective electrode 1 peripheral devices balance 7 manual dosing controller 2 printer 1. All coleparmer electrodes are doublejunction combination ion selective electrodes and are convenient to use in places where two electrodes wont fit. Go direct chloride ion selective electrode ise is used to measure the concentration of chloride cl. The electrode is designed for the detection of chloride ions cl in aqueous solutions and is suitable for use in both field and laboratory applications. In this case, the ion selective part is a solid substance in direct contact with the solution to be measured. This method is for the analysis of simple chloride ion rather than total chloride, as analysis using the ion selective electrode is not preceded by a distillation step.
The vernier chloride ion selective electrode is used to measure the concentration of chloride cl. The 8810 analyzer offers a new way of monitoring lowlevel chloride in power applications. Thermo orion chlorine electrode manual fondriest environmental. Silversulfide ion selective electrode user guide instrumart. All the consumables you need to measure fluoride or ammonia in water and wastewater are available with one part number. The hi4107 is a solid state, combination ion selective electrode ise for the determination of chloride cl in solution. Residual chlorine ion selective electrode user guide. Refer to the meter user guide for more specific information. The silver chloride sensing pellet produces a potential change due to the chloride ion exchange between the inorganic pellet membrane and the sample. These are general instructions that can be used with most meters to check the electrode operation. The chloride ion selective electrode you will use is a crystalline solidstate electrode that contains a membrane, as shown in the diagram below figure 1.
All electrodes include a 30ml bottle of reference solution, a reference filling pipette, 1m cable, bnc connector, and an instruction manual. Silversulfide ion selective electrode user guide 7 checking electrode operation slope these are general instructions that can be used with most meters to check the electrode operation. The main characteristic of a solid state electrode is that the sensing material is almost insoluble in water, meaning a. The vernier chloride ionselective electrode is used to measure the concentration of. The omega chloride ion electrode, ise8760, reference electrode. Multi kit detailed information dos and donts click here. This user guide contains information on the preparation, operation and maintenance of the thermo scientific orion single junction reference electrode, cat.
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